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研究生: 郭芳妤
Kuo, Fang Yu
論文名稱: 旋風分離器結合表面聲波感測器應用於PM2.5偵測
PM2.5 Detection by Surface Acoustic Wave Sensor with a Cyclone Separator
指導教授: 饒達仁
Yao, Da Jeng
口試委員: 林致廷
鄭桂忠
學位類別: 碩士
Master
系所名稱: 工學院 - 奈米工程與微系統研究所
Institute of NanoEngineering and MicroSystems
論文出版年: 2016
畢業學年度: 105
語文別: 中文
論文頁數: 88
中文關鍵詞: 旋風分離器表面聲波感測器PM2.5
外文關鍵詞: Cyclone Separator, Surface Acoustic Wave Sensor, PM2.5
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  • 本研究利用旋風分離器結合剪切式表面聲波( shear horizontal surface acoustic wave,SAW )原理發展出微型化的PM2.5感測系統,設計概念是將旋風分離器用於分離小於2.5微米之懸浮微粒,並輸送至表面聲波晶片上進行感測。利用離心管作為旋風分離器,可有效縮小裝置體積及流量需求;以36° YX-LiTaO3之壓電材料配合微機電之黃光微影製程完成感測晶片,搭配共振電路即可成功激發出中心頻率122MHz的表面聲波,並透過頻率變化量來判斷沉降於感測晶片上的微粒重量,進而計算出空氣中懸浮微粒之質量濃度( μg/m3 ),因此研究分為旋風分離器的效率設計、模擬以及表面聲波晶片量測兩個主要部分,最終進行裝置的整合實驗。
    設計可量測一般環境中PM2.5濃度的微型化感測器為本研究的最終目標,為達到此目標,將會對旋風分離器的耗能、裝置體積以及感測器靈敏度、穩定度等進行探討與改進。旋風分離器方面,利用市售的0.2ml離心管結合0.5毫米直徑大小的進、出氣口成為一旋風分離器,以CFD軟體進行效率模擬出粒徑截切點d50為2.5微米時,流量需求約是0.125LPM,搭配微型幫浦後的分離器體積大約是100cm3以下;表面聲波感測器方面,每1奈克的微粒會造成約9赫茲的頻率變化量,兩者結合進行PM2.5感測,計算後的濃度值與氣膠監視量測儀的濃度值有很強的正相關性,當採樣時間為160秒,感測最低濃度極限為11μg/m3,所需總感測時間約為5分鐘。


    In this research, a PM2.5 monitor prototype is designed and developed, including the shear horizontal mode surface acoustic wave (SH-SAW) sensor combining with a cyclone separator. In the experiments, aerosols generated by incense smoke will be separated and sampled inside the designed cyclone separator first, and the sampled PM2.5 will be introduced into the sensing area of SH-SAW chip for the detection. Microcentrifuge tubes as the cyclone separator can reduce the device size and power consumption effectively; 122 MHz surface acoustic wave (SAW) chips are fabricated by MEMS techniques in well design and processes; gold interdigital transducers are deposited on the 36° YX-LiTaO3 and using different frequency shift to identify the concentration of sample. Therefore the research is divided into two major parts: cyclone separator design, efficiency simulation and SAW chip detection experiment.
    To accomplish the goal of detecting the PM concentration in normal atmosphere, the efficiency, device size of the separator and the sensitivity, stability of the SAW chip will be discussed and improved. 0.2 mL microcentrifuge tube with 0.5mm inlet and outlet diameter as the separator has the separation cutoff diameters (d50) at 2.5μm, and the required inlet volumetric flow rate is 0.125 LPM simulated by CFD software; SAW sensor exhibits sensitivity approximately 9Hz/ng; PM2.5 detection experiment conducting with integrated device, shows the strong positive linear correlation between aerosol monitor data, the concentration limit of detection is 11μg/m3 with 160 seconds sample time, total detection time is 5 minutes.

    摘要 i Abstract ii 圖目錄 v 表目錄 vii 第一章 緒論 1 1.1研究動機 1 1.2 PM2.5簡介 3 1.3研究目標 7 第二章 文獻回顧 9 2.1PM2.5分離採樣器種類 9 2.1.1濾紙( Filter ) 9 2.1.2虛擬衝擊器( Virtual Impactor ) 10 2.1.3旋風分離器( Cyclone ) 11 2.2懸浮微粒感測器種類 13 2.2.1光散射式感測器 13 2.2.2電遷移率式感測器 14 2.2.3懸臂樑式感測器 15 2.2.4石英晶體微量天平 15 2.2.5表面聲波感測器 16 2.2.6其他懸浮微粒感測器及儀器 16 2.2.7各種懸浮微粒感測器之比較 17 2.3微機電技術應用於懸浮微粒感測文獻 19 第三章 表面聲波感測器原理 24 3.1表面聲波簡介 24 3.2壓電效應 27 3.3壓電材料種類及材料參數 30 3.2.1尤拉角( Euler-angle )及切面 31 3.2.2機電耦合係數( electromechanical coupling coefficient, K2 ) 32 3.2.3溫度延遲係數( temperature coefficient of delay,TCD ) 33 3.2.4壓電基材的插入損失( insertion loss,IL ) 34 3.4指叉式電極轉換器 37 3.5表面聲波元件感測機制 40 3.6懸浮微粒感測器指標 41 第四章 旋風分離器與感測系統設計 43 4.1旋風分離器設計與模擬 43 4.1.1旋風分離器設計參數 43 4.1.2分離效率 45 4.1.3分離效率模擬 46 4.2表面聲波晶片製備 50 4.2.1表面聲波晶片設計 50 4.1.2黃光微影製程 52 4.3量測方法與系統架設 55 4.3.1整體量測方法與系統 55 4.3.2微型腔體設計 59 4.3.4電路設計 60 4.3.3實驗所用之儀器 61 第五章 實驗結果 64 5.1旋風分離器效率模擬 64 5.2表面聲波感測器穩定性測試 69 5.2.1感測器中心頻率測量 69 5.2.2實驗環境穩定性測試 71 5.2.3電壓穩定性測試 72 5.3.4氣流穩定性測試 72 5.3懸浮微粒測量實驗結果 75 5.3.1表面聲波感測器靈敏度測試 76 5.3.2表面聲波感測器結合旋風分離器之測試 79 第六章 結論 83 未來工作 84 第七章 參考文獻 86

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