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研究生: 石家榮
Shih, Chia-Jung
論文名稱: 雙層淋幕式塗佈之分析
指導教授: 劉大佼
Liu, Ta-Jo
口試委員:
學位類別: 碩士
Master
系所名稱: 工學院 - 化學工程學系
Department of Chemical Engineering
論文出版年: 2010
畢業學年度: 98
語文別: 中文
論文頁數: 115
中文關鍵詞: 淋幕式塗佈雙層塗佈懸浮液
外文關鍵詞: curtain coating, two-phase coating, suspensions
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  • 在現今工業上,多相塗佈製程已是不可或缺的重要製程之一,本研究以淋幕式塗佈為實驗系統探討微粒子添加入甘油水溶液後,塗佈行為的變化,並研究雙層淋幕式塗佈在不同參數下塗佈之行為。單層淋幕式塗佈實驗結果顯示,添加微粒子於甘油水溶液中,可以有助於降低最小成膜流量和穩定動態濕潤線,抑制空氣滲入,提高最大塗佈速度,且粒子濃度越高,粒徑越小延後空氣滲入的效果越好。雙層淋幕式塗佈實驗發現,透過攜帶層的幫助,可以提高上層塗液的最大塗佈速度,且攜帶層中粒子的含量越高,越有助於提升上層塗液的最大塗佈速度,再透過改變上下層的黏度比以及攜帶層的流量等參數,發現改變攜帶層的流量對上層塗液的最大塗佈速度並不會造成影響,而利用較低黏度的攜帶層則會有助於提升上層的最大塗佈速度,且上下層間的黏度會存在一最佳黏度比,如果上下層黏度相差太大,則會造成淋幕的不穩。


    摘要 I 總目錄 II 圖目錄 V 1. 第一章、緒論 1 1-1 背景說明 1 1-2 塗佈技術簡介 2 1-3 淋幕式塗佈 5 1-4 多層式塗佈技術 7 1-5 研究目的 12 2. 第二章、文獻回顧 15 2-1 淋幕式塗佈工程 (curtain coating) 15 2-2 雙層塗佈技術 (two-layered coating) 28 2-3 膠體懸浮液 (suspension) 30 3. 第三章、實驗方法 37 3-1 實驗儀器 38 3-2 分析儀器 44 3-3 實驗藥品 47 3-4 實驗步驟 49 3-4.1 塗液配置方式 49 3-4.2 物性測量方法 50 3-4.3 塗佈實驗機構架設與步驟 52 3-4.4 塗佈視窗上下限判定 61 4. 第四章、實驗結果與討論 64 4-1 流體基礎物性分析 64 4-1.1 單層淋幕式塗佈實驗之塗液物性 64 4-1.2雙層淋幕式塗佈實驗之塗液物性 66 4-2 單層淋幕式塗佈之研究 67 4-2.1 PMMA粒子粒徑對塗佈視窗之影響 67 4-2.2 PMMA粒子濃度對塗佈視窗之影響 72 4-2.3 粒子效應對不同濃度甘油的塗佈視窗之影響 74 4-2.4 在高邊桿下粒子效應對塗佈視窗之影響 75 4-2.5 結果與討論 79 4-3 雙層淋幕式塗佈之研究 96 4-3.1 微粒子之影響 96 4-3.2 黏度比之影響 97 4-3.3 攜帶層流量之影響 99 4-3.4 結果與討論 100 附錄、參考文獻 112

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