本論文主要分為兩部份，第一部份研究以鈦、鎳及鈦、鎳、銅真空反應放熱特性作304不□鋼、中碳鋼及Ti-6Al-4V鈦合金之真空硬銲。實驗結果顯示，鈦/鎳銲材原子比率不同，會造成304不□鋼及中碳鋼硬銲試片接合面金相組織的變化，當鈦/鎳原子比率愈高真空反應放熱之熱量愈大，而銲接區內愈容易生成硬脆的相；以Monel 400鎳銅箔作銲材來硬銲Ti-6Al-4V鈦合金試片在900℃8min的真空硬銲條件下可以成功銲合，而隨著硬銲溫度增加，試片費德曼組織增加。
本文第二部份研究添加微量鈦鎳銅三元混合粉末於鉬粉中燒結，對鉬燒結成品性質的影響。實驗結果顯示，鈦鎳銅三元粉末添加，有助於鉬燒結試片的緻密度及晶粒成長；但添加鈦鎳銅三元粉末中鈦含量增加，則鉬燒結試片二次相增加，鈦元素聚集在二次相中導致燒結試片暫態液相量減少，燒結試片晶粒不易成長，緻密度變差，硬度值較小。

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