本論文主要是利用有機催化劑的方式，來催化成長奈米碳管，不同的過渡金屬催化劑會表現出不同之效果，而同一種催化劑亦會因為一些外在環境狀況的不同而有不同之催化能力。
在本論文中，利用鑽石做為成長奈米碳管(碳纖維)的碳源，這裡的鑽石包括了鑽石粉末以及鑽石膜兩種。在含有鑽石的基材上添加催化劑(過渡金屬元素)來成長奈米碳管(碳纖維)。在取得的鑽石膜和購買的奈米鑽石粉末試片分別濺鍍上鐵鈷合金和旋鍍上有機催化劑，最後置於900℃以上的高溫中退火形成奈米碳管(碳纖維)，再進行特性的研究。本研究將更進一步評估黃光微影製程來做奈米碳管(碳纖維)的選區成長。
成長出來的奈米碳管(碳纖維)其外徑大部分為10奈米至30奈米之間，且其管壁上方皆可發現有催化劑，催化劑顆粒的大小與管徑成正相關。利用鑽石膜所成長出的奈米碳纖維較短且直；而奈米鑽石粉末所成長出的奈米碳纖維則較長且彎曲。
鑽石退火後其場發射有增強的現象，這應該是因為奈米碳纖維的場發射較鑽石因負電子親和力所產生的場發射特性好，故推論奈米碳管(碳纖維)的形成有助於場發射特性的提升。

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