揮發性有機化合物是近十年來普遍被認為是影響土壤、空氣、水源及人體健康的一種污染物質。隨著工業化的發展許多的物質或是使用這些物質已經被證實可釋放出揮發性有機化合物，這些物質如汽油產品、有機溶劑、染料及黏著劑等。透過使用這些物質則有助於揮發性有機化合物釋放於環境中，或者因為人們的不當使用也是導致這些污染物逸散的原因之一。然而，藉由檢測這類物質的逸散濃度，可使我們瞭解環境遭受污染的程度，也可以進一步採取必要的整治或是預防措施。因此本論文發展氣相層析質譜及電子鼻技術應用於檢測油品洩漏及運動鞋類中揮發性有機化合物分析。本論文共分成四章：
一.緒論
二.建立氣相層析質譜與主成分分析技術以鑑定地下汽油儲槽洩漏
三.使用電子鼻做為油品洩漏及非法油行油品之快速檢測及使用氣相層析質譜儀確認
四.利用吸附管熱脫附法結合氣相層析質譜儀鑑定鞋材中逸散的揮發性有機化合物
第二章為使用氣相層析質譜分析技術於檢測台灣地區站齡超過十年以上加油站其地下汽油儲槽之洩漏情形，並以主成分分析法預測可能洩漏之地下油槽。第三章為運用電子鼻分析技術進行油品洩漏之判定，並以氣相層析質譜儀進行確認。第四章則利用氣相層析質譜分析鞋材中逸散之揮發性有機化合物濃度，及探討鞋材重量與逸散濃度之相互關係。

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